反应条件
1: methyllithium With B-OMe-9-borabicyclo[3.3.1]nonane in tetrahydrofuran T=-78 - 20°C; Methylation; 1 h; 2: 4-iodobenzene-1-sulphonic acid With barium dihydroxide; triphenyl-arsane; bis(benzonitrile)palladium(II) dichloride in tetrahydrofuran; N,N-dimethyl-formamide T=20°C; Suzuki reaction; 0.5 h;
参考文献
Braun, Matthew P.; Dean, Dennis C.; Melillo, David G.
Journal of Labelled Compounds and Radiopharmaceuticals, 1999 , vol. 42, # 5 p. 469 - 476
