alpha,alpha'-二乙基-4,4'-二甲氧基二苯乙烯合成路线 (共 62 条)
反应条件
propan-1-ol; diethyl ether
T=0°C;
参考文献
Gerber; Curtin
Journal of the American Chemical Society, 1949 , vol. 71, p. 1499
反应条件
phosphorus tribromide
T=100°C;
参考文献
Squibb and Sons
Patent: US2252696 , 1939 ;
反应条件
propan-1-ol; diethyl ether
参考文献
Gerber; Curtin
Journal of the American Chemical Society, 1949 , vol. 71, p. 1499
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Mustafa
Journal of the Chemical Society, 1951 , p. 1370
反应条件
1: SOCl2; pyridine; benzene / durch Behandeln des hergestellten Saeurechlorids mit Anisol und SnCl4 in Benzol
2: diethyl ether; benzene
3: boron chloride diethyl etherate; tetrachloromethane / 20 °C
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参考文献
Wilds; Biggerstaff
Journal of the American Chemical Society, 1945 , vol. 67, p. 789,791
反应条件
1: 56 percent / sodium iodide; iodine monochloride / CH2Cl2 / 14 h / 0 - 20 °C
2: 12 percent / NaHCO3; water / Pd(PPh3)4 / dimethylformamide / 100 °C
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参考文献
Henaff, Nadine; Whiting, Andrew
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 3 p. 395 - 400
反应条件
1: N,N-dimethyl-aniline; thionyl chloride
2: TiCl4 / Behandeln des Reaktionsprodukts mit Jod in CHCl3
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参考文献
Sisido et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 3591
反应条件
titanium tetrachloride
Behandeln des Reaktionsprodukts mit Jod in CHCl3;
参考文献
Sisido et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 3591
参考文献
Reid; Wilson
Journal of the American Chemical Society, 1942 , vol. 64, p. 1625
反应条件
titanium tetrachloride; zinc in tetrahydrofuran
20 h; Heating; Yields of byproduct given;
参考文献
Leimner, Juergen; Weyerstahl, Peter
Chemische Berichte, 1982 , vol. 115, # 12 p. 3697 - 3705
反应条件
toluene; trichlorophosphate
T=100°C;
参考文献
Chinoin
Patent: DE717653 , 1939 ;
DRP/DRBP Org.Chem.
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Foeldi; Demjen
Chemische Berichte, 1941 , vol. 74, p. 930,933