1-甲氧基-4-[4-(4-甲氧基苯基)己烷-3-基]苯合成路线 (共 35 条)
反应条件
palladium on activated charcoal; acetone Hydrogenation;
参考文献
Docken; Spielman
Journal of the American Chemical Society, 1940 , vol. 62, p. 2163
反应条件
nickel; Petroleum ether T=75 - 80°C; weiteres Reagens: Wasser; unter Abdestillieren des Petrolaethers;
参考文献
Sisido et al.
Journal of Organic Chemistry, 1949 , vol. 14, p. 1124,1126
Rep. Inst. chem. Res. Kyoto Univ.Chem.Abstr., 1949 , vol. 18, p. 15
Rep. Inst. chem. Res. Kyoto Univ.Chem.Abstr., 1951 , p. 7553
反应条件
diacetyl peroxide T=145°C;
参考文献
Kharasch; McBay; Urry
Journal of Organic Chemistry, 1945 , vol. 10, p. 401,404
反应条件
diethyl ether T=30°C;
参考文献
Wilds; McCormack
Journal of Organic Chemistry, 1949 , vol. 14, p. 45,57
反应条件
1: glacial acetic acid; palladium / Hydrogenation 2: aqueous NaOH View Scheme
参考文献
Dodds et al.
Proceedings of the Royal Society of London, Series B: Biological Sciences, 1939 , vol. 127, p. 140,153 Anm. 154
Proceedings of the Royal Society of London, 1944 , vol. 132, p. 83,91
反应条件
1: diethyl ether; benzene 2: KHSO4 / 195 - 200 °C 3: ethanolic KOH / 200 - 210 °C 4: acetone; palladium/charcoal / Hydrogenation 5: aqueous NaOH View Scheme
参考文献
Dodds et al.
Proceedings of the Royal Society of London, Series B: Biological Sciences, 1939 , vol. 127, p. 140,153 Anm. 154
Proceedings of the Royal Society of London, 1944 , vol. 132, p. 83,91
反应条件
1: petroleum ether; HBr / <0 2: diethyl ether; CoCl2 / 30 °C View Scheme
参考文献
Kharasch; McBay; Urry
Journal of Organic Chemistry, 1945 , vol. 10, p. 401,404
反应条件
hydrogen sulfide T=305 - 310°C;
参考文献
Peak; Short
Journal of the Chemical Society, 1943 , p. 232
参考文献
v. Wessely; Welleba
Chemische Berichte, 1941 , vol. 74, p. 777,782
Full Text Show Details
Dodds et al.
Proceedings of the Royal Society of London, Series B: Biological Sciences, 1939 , vol. 127, p. 140,153 Anm. 154
Proceedings of the Royal Society of London, 1944 , vol. 132, p. 83,91
反应条件
1: KHSO4 / 195 - 200 °C 2: ethanolic KOH / 200 - 210 °C 3: acetone; palladium/charcoal / Hydrogenation 4: aqueous NaOH View Scheme
参考文献
Dodds et al.
Proceedings of the Royal Society of London, Series B: Biological Sciences, 1939 , vol. 127, p. 140,153 Anm. 154
Proceedings of the Royal Society of London, 1944 , vol. 132, p. 83,91