S-(三氟甲基)二苯并噻吩三氟甲基磺酸盐合成路线 (共 67 条)
反应条件
2,4,6-trimethyl-pyridine; copper diacetate in N,N-dimethyl acetamide
T=25°C; P=760.051 Torr; 16 h; Inert atmosphere;
参考文献
Xu, Jun; Luo, Dong-Fen; Xiao, Bin; Liu, Zhao-Jing; Gong, Tian-Jun; Fu, Yao; Liu, Lei
Chemical Communications, 2011 , vol. 47, # 14 p. 4300 - 4302
反应条件
(C6H5)BCat; potassium hydride
1.) THF, r.t., 1 h; -78 deg C, 1 h, 2.) -78 to 0 deg C, 2.5 h; Yield given. Multistep reaction;
参考文献
Umemoto, Teruo; Adachi, Kenji
Journal of Organic Chemistry, 1994 , vol. 59, # 19 p. 5692 - 5699
反应条件
in tetrahydrofuran
-78 deg C to r.t.;
参考文献
Umemoto; Ishihara
Tetrahedron Letters, 1990 , vol. 31, # 25 p. 3579 - 3582
反应条件
copper in acetonitrile
T=60°C; 9 h; Inert atmosphere;
参考文献
Zhu, Lingui; Liu, Shasha; Douglas, Justin T.; Altman, Ryan A.
Chemistry - A European Journal, 2013 , vol. 19, # 38 p. 12800 - 12805
反应条件
copper in acetonitrile
T=60°C; 9 h; Inert atmosphere;
参考文献
Zhu, Lingui; Liu, Shasha; Douglas, Justin T.; Altman, Ryan A.
Chemistry - A European Journal, 2013 , vol. 19, # 38 p. 12800 - 12805
反应条件
2,4,6-trimethyl-pyridine; copper diacetate in N,N-dimethyl acetamide
T=0°C; P=760.051 Torr; 16 h; Inert atmosphere;
参考文献
Xu, Jun; Luo, Dong-Fen; Xiao, Bin; Liu, Zhao-Jing; Gong, Tian-Jun; Fu, Yao; Liu, Lei
Chemical Communications, 2011 , vol. 47, # 14 p. 4300 - 4302
反应条件
2,4,6-trimethyl-pyridine; copper diacetate in N,N-dimethyl acetamide
T=25°C; P=760.051 Torr; 16 h; Inert atmosphere;
参考文献
Xu, Jun; Luo, Dong-Fen; Xiao, Bin; Liu, Zhao-Jing; Gong, Tian-Jun; Fu, Yao; Liu, Lei
Chemical Communications, 2011 , vol. 47, # 14 p. 4300 - 4302
反应条件
copper in acetonitrile
T=60°C; 9 h; Inert atmosphere;
参考文献
Zhu, Lingui; Liu, Shasha; Douglas, Justin T.; Altman, Ryan A.
Chemistry - A European Journal, 2013 , vol. 19, # 38 p. 12800 - 12805
反应条件
copper in acetonitrile
T=60°C; 9 h; Inert atmosphere;
参考文献
Zhu, Lingui; Liu, Shasha; Douglas, Justin T.; Altman, Ryan A.
Chemistry - A European Journal, 2013 , vol. 19, # 38 p. 12800 - 12805
反应条件
2,4,6-trimethyl-pyridine; copper diacetate in N,N-dimethyl acetamide
T=0°C; P=760.051 Torr; 16 h; Inert atmosphere;
参考文献
Xu, Jun; Luo, Dong-Fen; Xiao, Bin; Liu, Zhao-Jing; Gong, Tian-Jun; Fu, Yao; Liu, Lei
Chemical Communications, 2011 , vol. 47, # 14 p. 4300 - 4302