S-(三氟甲基)二苯并噻吩三氟甲基磺酸盐合成路线 (共 67 条)
反应条件
2,4,6-trimethyl-pyridine; copper diacetate in N,N-dimethyl acetamide T=25°C; P=760.051 Torr; 16 h; Inert atmosphere;
参考文献
Xu, Jun; Luo, Dong-Fen; Xiao, Bin; Liu, Zhao-Jing; Gong, Tian-Jun; Fu, Yao; Liu, Lei
Chemical Communications, 2011 , vol. 47, # 14 p. 4300 - 4302
反应条件
2,4,6-trimethyl-pyridine; copper diacetate in N,N-dimethyl acetamide T=25°C; P=760.051 Torr; 16 h; Inert atmosphere;
参考文献
Xu, Jun; Luo, Dong-Fen; Xiao, Bin; Liu, Zhao-Jing; Gong, Tian-Jun; Fu, Yao; Liu, Lei
Chemical Communications, 2011 , vol. 47, # 14 p. 4300 - 4302
反应条件
4-(N,N-dimethlyamino)pyridine in N,N-dimethyl-formamide T=0°C; 2 h;
参考文献
Tetrahedron Letters, , vol. 31, # 25 p. 3579 - 3582
反应条件
pyridine in N,N-dimethyl-formamide T=80°C;
参考文献
Umemoto; Ishihara
Tetrahedron Letters, 1990 , vol. 31, # 25 p. 3579 - 3582
反应条件
(C6H5)BCat; potassium hydride 1.) THF, r.t., 1 h; -78 deg C, 1 h, 2.) -78 to 0 deg C, 2.5 h; Yield given. Multistep reaction;
参考文献
Umemoto, Teruo; Adachi, Kenji
Journal of Organic Chemistry, 1994 , vol. 59, # 19 p. 5692 - 5699
反应条件
nitronium trifluoromethanesulfonate 72 h; Ambient temperature;
参考文献
Umemoto, Teruo; Ishihara, Sumi
Journal of the American Chemical Society, 1993 , vol. 115, # 6 p. 2156 - 2164
反应条件
sulfuric acid T=40°C; 5.5 h;
参考文献
Umemoto, Teruo; Ishihara, Sumi; Adachi, Kenji
Journal of Fluorine Chemistry, 1995 , vol. 74, # 1 p. 77 - 82
反应条件
2,4,6-trimethyl-pyridine; copper diacetate in N,N-dimethyl acetamide T=20°C; 20 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 47, # 14 p. 4300 - 4302
反应条件
2,4,6-trimethyl-pyridine in N,N-dimethyl acetamide T=20°C; 20 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 47, # 14 p. 4300 - 4302
反应条件
(2R,6S)-2,6-dimethylpiperidine in 1,2-dichloro-ethane T=20°C; 20 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 47, # 14 p. 4300 - 4302