5-(三氟甲基)二苯并[b,d]硒吩鎓三氟甲烷磺酸酯合成路线 （共 8 条）
反应条件
fluorine in monofluoro-trichloromethane T=-35°C;
参考文献
Umemoto, Teruo; Ishihara, Sumi
Journal of the American Chemical Society, 1993 , vol. 115, # 6 p. 2156 - 2164
反应条件
in 1,2,2-trifluoro-trichloroethane 2 h; 0 deg C to r.t.;
参考文献
Umemoto, Teruo; Ishihara, Sumi
Journal of the American Chemical Society, 1993 , vol. 115, # 6 p. 2156 - 2164
反应条件
1: 67 percent / NaBH4 / dimethylformamide / -30 - 20 °C 2: 76 percent / F2 / CCl3F / -35 °C View Scheme
参考文献
Umemoto; Ishihara
Tetrahedron Letters, 1990 , vol. 31, # 25 p. 3579 - 3582
反应条件
1: 85 percent / m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature 2: 94 percent / 1,1,2-trichloro-1,2,2-trifluoro-ethane / 2 h / Ambient temperature View Scheme
参考文献
Umemoto; Ishihara
Tetrahedron Letters, 1990 , vol. 31, # 25 p. 3579 - 3582
反应条件
in N,N-dimethyl-formamide 20 h; Ambient temperature;
参考文献
Umemoto; Ishihara
Tetrahedron Letters, 1990 , vol. 31, # 25 p. 3579 - 3582
反应条件
in N,N-dimethyl-formamide 20 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 31, # 25 p. 3579 - 3582
反应条件
(C6H5)BCat; potassium hydride 1.) THF, r.t., 1 h; -78 deg C, 1 h, 2.) -78 to 0 deg C, 2.5 h; Yield given. Multistep reaction;
参考文献
Umemoto, Teruo; Adachi, Kenji
Journal of Organic Chemistry, 1994 , vol. 59, # 19 p. 5692 - 5699
反应条件
in tetrahydrofuran
-78 deg C to r.t.;
参考文献
Umemoto; Ishihara
Tetrahedron Letters, 1990 , vol. 31, # 25 p. 3579 - 3582
