hydrogen; palladium 10 on activated carbon in methanol T=26°C; P=2068.65 Torr; 2 h;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3903058', constants.ctx, '0')">boron tribromide</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=-70 - 0&deg;C;&nbsp;<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: sodium tetrahydroborate / N,N-dimethyl-formamide; methanol / 2.33 h / 0 - 10 &deg;C<br />2: boron tribromide / dichloromethane / -70 - 0 &deg;C<br /> <br /> &nbsp;