in benzene treatment of the Zr compd. in benzene suspn. with SbCl2Br (1 equiv) (25°C), removal of solvent (vac.); extn. (hexane/ether (10:1)), chromy. (anhyd. MgSO4);
参考文献
Buchwald, Stephen L.; Fisher, Richard A.; Davis, William M.
Organometallics, 1989 , vol. 8, p. 2082 - 2084
in benzene treatment of the Zr compd. in benzene suspn. with PhSbCl2 (1 equiv) (25°C), removal of solvent (vac.); extn. (hexane/ether (10:1)), chromy. (alumina III);
参考文献
Buchwald, Stephen L.; Fisher, Richard A.; Davis, William M.
Organometallics, 1989 , vol. 8, p. 2082 - 2084
in benzene treatment of the Zr compd. in benzene suspn. with PhSbCl2 (1 equiv) (25°C), removal of solvent (vac.); extn. (hexane/ether (10:1)), chromy. (alumina III);
参考文献
Buchwald, Stephen L.; Fisher, Richard A.; Davis, William M.
Organometallics, 1989 , vol. 8, p. 2082 - 2084