3,4,9,10-苝四羧酸二酐合成路线 (共 71 条)
反应条件
sulfuric acid; bromine; iodine
T=85°C; 24.5 h;
参考文献
Keerthi, Ashok; Valiyaveettil, Suresh
Journal of Physical Chemistry B, 2012 , vol. 116, # 15 p. 4603 - 4614
反应条件
sulfuric acid; bromine; iodine
T=85°C; 18 h;
参考文献
Naidu, Jaishri J.; Shin, Seunghan; Jeong, Kwang-Un; Lee, Myong-Hoon
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 9 p. 2705 - 2708
参考文献
Popovic, Zoran D.; Loutfy, Rafik O.; Hor, Ah-Mee
Canadian Journal of Chemistry, 1985 , vol. 63, p. 134 - 139
Title/Abstract Full Text Show Details
Shi, Min-Min; Chen, Hong-Zheng; Shi, Yue-Wen; Sun, Jing-Zhi; Wang, Mang
Journal of Physical Chemistry B, 2004 , vol. 108, # 19 p. 5901 - 5904
反应条件
potassium hydroxide
T=210°C;
参考文献
Zieger,H.E.
Journal of Organic Chemistry, 1966 , vol. 31, p. 2977 - 2981
反应条件
1: aq. KOH / 210 °C
2: SOCl2
3: (i) Mg, CdCl2, (ii) /BRN= 2592275/
4: N2H4*H2O, KOH, triethylene glycol
View Scheme
参考文献
Zieger,H.E.
Journal of Organic Chemistry, 1966 , vol. 31, p. 2977 - 2981
反应条件
in N,N-dimethyl-formamide
4 h; Reflux;
参考文献
Perrin, Lara; Hudhomme, Pietrick
European Journal of Organic Chemistry, 2011 , # 28 p. 5427 - 5440
反应条件
in water
T=60°C; 3.5 h;
参考文献
Nagao, Yukinori; Misono, Takahisa
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 4 p. 1191 - 1194
反应条件
in various solvent(s)
T=202°C; Condensation; 0.5 h;
参考文献
Aroca; Constantino; Duff, James
Applied Spectroscopy, 2000 , vol. 54, # 8 p. 1120 - 1125
→
41635-87-4菲并[2'',1'',10'':4,5,6;7'',8'',9'':4',5',6']二异喹啉并[2,1-a:2',1'-a']二萘嵌间二氮杂苯-8,13-二酮+
反应条件
piperazine; phenol
T=70 - 180°C; 8 h; Melt;
参考文献
Mamada, Masashi; Perez-Bolivar, Cesar; Anzenbacher, Pavel
Organic Letters, 2011 , vol. 13, # 18 p. 4882 - 4885
反应条件
potassium hydroxide in water
12 h; Heating;
参考文献
Takahashi, Masaki; Suzuki, Yousuke; Ichihashi, Yasunori; Yamashita, Mitsuji; Kawai, Hideki
Tetrahedron Letters, 2007 , vol. 48, # 3 p. 357 - 359