3,4,9,10-苝四羧酸二酐合成路线 （共 71 条）
反应条件
zinc diacetate; 3-methyl-phenol 12 h; Heating;
参考文献
Neuber, Christian; Baete, Markus; Giesa, Reiner; Schmidt, Hans-Werner
Journal of Materials Chemistry, 2006 , vol. 16, # 34 p. 3466 - 3477
反应条件
1.1: propan-1-ol; water / 12 h / 65 °C / Inert atmosphere 2.1: sulfuryl dichloride; iodobenzene; iodine / nitrobenzene / 14 h / 80 °C / Inert atmosphere 2.2: 6 h / Inert atmosphere 3.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 6 h / 160 °C / Inert atmosphere 4.1: potassium hydroxide / water; isopropyl alcohol / 24 h / Inert atmosphere; Reflux View Scheme
参考文献
Perrin, Lara; Hudhomme, Pietrick
European Journal of Organic Chemistry, 2011 , # 28 p. 5427 - 5440
反应条件
sulfuric acid; chlorine T=120°C;
参考文献
Journal of the American Chemical Society, , vol. 130, # 26 p. 8271 - 8279
反应条件
chlorosulfonic acid; iodine T=70°C; 5 h;
参考文献
Tetrahedron, , vol. 68, # 2 p. 722 - 729
反应条件
chlorosulfonic acid; iodine T=70°C; 20 h;
参考文献
Tetrahedron, , vol. 68, # 2 p. 722 - 729
反应条件
1: With sulfuric acid
T=20°C; 2 h;
2: With bromine; iodine
T=80 - 100°C; 4 - 6 h;
参考文献
UNIVERSITA 'DEGLI STUDI DI ROMA "LA SAPIENZA"
Patent: WO2008/126123 A2, 2008 ;
Location in patent: Page/Page column 15; 19-20 ;
反应条件
sulfuric acid; bromine
T=40°C; 12 h;
参考文献
Zhou, Erjun; Tajima, Keisuke; Yang, Chunhe; Hashimoto, Kazuhito
Journal of Materials Chemistry, 2010 , vol. 20, # 12 p. 2362 - 2368
反应条件
sulfuric acid; bromine
T=85°C;
参考文献
Jiang, Wei; Li, Yan; Yue, Wan; Zhen, Yonggang; Qu, Jianqiang; Wang, Zhaohui
Organic Letters, 2010 , vol. 12, # 2 p. 228 - 231
反应条件
1: With sulfuric acid; iodine
T=20°C; 2 h;
2: With bromine
T=80°C; 18 h;
参考文献
Choi, Jun; Sakong, Chun; Choi, Jae-Hong; Yoon, Chun; Kim, Jae Pil
Dyes and Pigments, 2011 , vol. 90, # 1 p. 82 - 88
反应条件
1: With sulfuric acid
T=20°C; 12 h;
2: With bromine; iodine
T=85 - 110°C; Title compound not separated from byproducts;
参考文献
Queste, Mathieu; Cadiou, Cyril; Pagoaga, Bernard; Giraudet, Louis; Hoffmann, Norbert
New Journal of Chemistry, 2010 , vol. 34, # 11 p. 2537 - 2545
