3,4,9,10-苝四羧酸二酐合成路线 （共 71 条）
反应条件
zinc diacetate in various solvent(s) T=220°C; 4 h; further reagents: Pb(OAc)2, HOAc;
参考文献
Chemische Berichte, , vol. 118, # 11 p. 4641 - 4645
反应条件
1H-imidazole; zinc diacetate; water T=190°C; 23 h;
参考文献
Liebigs Annalen, , # 7 p. 1229 - 1244
反应条件
zinc diacetate in quinoline T=180 - 230°C; Yield given;
参考文献
Rademacher, Andreas; Maerkle, Suse; Langhals, Heinz
Chemische Berichte, 1982 , vol. 115, # 8 p. 2927 - 2934
反应条件
1.1: iodine; H2SO4 / 2 h / 20 °C 1.2: bromine; H2SO4 / 18 h / 80 °C 2.1: 46 g / acetic acid / 1-methyl-pyrrolidin-2-one / 120 h / 120 °C View Scheme
参考文献
Ramanan, Charusheela; Smeigh, Amanda L.; Anthony, John E.; Marks, Tobin J.; Wasielewski, Michael R.
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 386 - 397
反应条件
1: perylene-3,4,9,10-tetracarboxylic dianhydride With sulfuric acid; iodine T=20°C; 2 h; Inert atmosphere; 2: With bromine T=80°C; 18 h; 3: 2,6-bis(1-methylethyl)benzenamine With acetic acid in 1-methyl-pyrrolidin-2-one T=120°C; 96 h;
参考文献
Choi, Jun; Sakong, Chun; Choi, Jae-Hong; Yoon, Chun; Kim, Jae Pil
Dyes and Pigments, 2011 , vol. 90, # 1 p. 82 - 88
反应条件
1: perylene-3,4,9,10-tetracarboxylic dianhydride With bromine 2: 2,6-bis(1-methylethyl)benzenamine With propionic acid T=155°C; 22 h;
参考文献
Bagui, Mahuya; Dutta, Tanmoy; Chakraborty, Sanjiban; Melinger, Joseph S.; Zhong, Haizhen; Keightley, Andrew; Peng, Zhonghua
Journal of Physical Chemistry A, 2011 , vol. 115, # 9 p. 1579 - 1592
反应条件
1: perylene-3,4,9,10-tetracarboxylic dianhydride With sulfuric acid T=20°C; 12 h; 2: With iodine T=20 - 85°C; 0.5 h; 3: 2,6-bis(1-methylethyl)benzenamine Further stages;
参考文献
Jiang, Wei; Li, Yan; Yue, Wan; Zhen, Yonggang; Qu, Jianqiang; Wang, Zhaohui
Organic Letters, 2010 , vol. 12, # 2 p. 228 - 231
反应条件
ammonium molibdate in N-methylpyrrolidone (NMP) T=198 - 202°C; 21 h; Product distribution / selectivity;
参考文献
SUN CHEMICAL CORPORATION
Patent: US2008/139813 A1, 2008 ;
Location in patent: Page/Page column 3 ;
反应条件
ammonium hydroxide in water T=90°C; 2 h;
参考文献
Yang, Lanying; Shi, Minmin; Wang, Mang; Chen, Hongzheng
Tetrahedron, 2008 , vol. 64, # 22 p. 5404 - 5409
反应条件
1: potassium hydroxide 2: ammonia View Scheme
参考文献
Ringk, Andreas; Li, Xiaoran; Gholamrezaie, Fatemeh; Smits, Edsger C. P.; Neuhold, Alfred; Moser, Armin; Van Der Marel, Cees; Gelinck, Gerwin H.; Resel, Roland; De Leeuw, Dago M.; Strohriegl, Peter
Advanced Functional Materials, 2013 , vol. 23, # 16 p. 2016 - 2023
