6,6-二甲基二环[3.1.1]庚-2-烯-2-乙醇合成路线 （共 13 条）
反应条件
Zn(BiO3)2 in toluene 2.5 h; Heating;
参考文献
Firouzabadi, Habib; Mohammadpour-Baltork, Iraj
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 4 p. 1131 - 1134
反应条件
iron(III) phosphate in acetonitrile
T=80°C; Prins condensation; 4 h;
参考文献
Pillai, Unnikrishnan R; Sahle-Demessie, Endalkachew
Chemical communications (Cambridge, England), 2004 , # 7 p. 826 - 827
反应条件
zirconia pillared zirconium phosphate ZrO2-ZrP-a-150 in toluene
T=80°C; 4 h; Reagent/catalyst;
参考文献
Wang, Xueyan; Wang, Tao; Hua, Weiming; Yue, Yinghong; Gao, Zi
Catalysis Communications, 2014 , vol. 43, p. 97 - 101
反应条件
lithium aluminium tetrahydride
参考文献
Ashcroft, Martyn R.; Bougeard, Peter; Bury, Adrian; Cooksey, Christopher J.; Johnson, Michael D.
Journal of Organometallic Chemistry, 1985 , vol. 289, p. 403 - 416
反应条件
lithium aluminium tetrahydride; sodium acetate; acetic acid
1.) 70 deg C, 12 h, 2.) ether; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Vyglazov, O. G.; Urbanovich, T. R.; Manukov, E. N.; Chuiko, V. A.; Udarov, B. G.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 101 p. 1896 - 1900
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 10 p. 2100 - 2104
反应条件
1: 180 - 220 °C
2: (saponification)
View Scheme
参考文献
Watanabe,S.
Bulletin of the Chemical Society of Japan, 1965 , vol. 38, p. 1231 - 1235
反应条件
lithium aluminium tetrahydride; sodium acetate; acetic acid
Mechanism;
参考文献
Vyglazov, O. G.; Urbanovich, T. R.; Manukov, E. N.; Chuiko, V. A.; Udarov, B. G.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 101 p. 1896 - 1900
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 10 p. 2100 - 2104
参考文献
Gupta, B. Dass; Das, Indira; Dixit, Vandana
Journal of Chemical Research, Miniprint, 1992 , # 9 p. 2409 - 2446
反应条件
acetic acid in methanol
T=62.5°C;
参考文献
Giddings, Rodney M.; Jones-Parry, Richard; Owen, Rawson; Whittaker, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 1525 - 1528
反应条件
acetic acid in methanol
T=62.5°C;
参考文献
Giddings, Rodney M.; Jones-Parry, Richard; Owen, Rawson; Whittaker, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 1525 - 1528
