2,6-二叔丁基-4-甲基苯酚合成路线 （共 290 条）
反应条件
n-butyllithium in tetrahydrofuran; hexane
1.) RT, overnight; 2.) 6 h, reflux;
参考文献
Haener,R.; Laube,T.; Seebach,D.
Journal of the American Chemical Society, 1985 , vol. 107, p. 5396
反应条件
(i) MnO2, toluene, (ii) /BRN= 102415/, Et2O; Multistep reaction;
参考文献
Woolhouse,A.D.
Australian Journal of Chemistry, 1977 , vol. 30, p. 1145 - 1152
反应条件
sodium hydroxide in water
参考文献
Roehm GmbH Chemische Fabrik Patentabteilung
Patent: US5424472 A1, 1995 ;
反应条件
sulfuric acid; sodium nitrite
T=-10 - -5°C; 0.25 h;
参考文献
Shpinel', Ya.I.; Klimova, I.V.; Belyaev, E.Yu.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 7 p. 1309 - 1312
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 7 p. 1493 - 1497
反应条件
phosphoric acid trimethyl ester; chlorine
T=80°C;
参考文献
Pearson; Donald E.
Patent: US3988369 A1, 1976 ;
反应条件
aluminium trichloride in tetrachloromethane
1 h; Ambient temperature;
参考文献
Shatskaya, T. A.; Gal'pern, M. G.; Skvarchenko, V. R.; Luk'yanets, E. A.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 2 p. 392 - 397,341 - 345
反应条件
potassium permanganate in dichloromethane
参考文献
Benjamin,B.M. et al.
Journal of Organic Chemistry, 1978 , vol. 43, # 15 p. 2986 - 2991
反应条件
sodium hydroxide; sodium sulfate in dichloromethane
参考文献
Hamari Chemicals, Ltd.
Patent: US4670607 A1, 1987 ;
反应条件
1: N-bromosuccinmide
2: diethyl ether / 20 °C
View Scheme
参考文献
Andriyashin; Bakhtiyarova; Cherkasov; Galkin; Galkina
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 12 p. 1576 - 1577
反应条件
in various solvent(s)
T=18.9 - 79.9°C; ΔE(excit); KineticsRate constant;
参考文献
Rousseau-Richard, Claire; Richard, Claude; Martin, Rene
Journal de Chimie Physique et de Physico-Chimie Biologique, 1989 , vol. 86, # 9 p. 2057 - 2066
