二甲基二硫代氨基甲酸钠合成路线 (共 123 条)
反应条件
sodium hydroxide in water T=20°C; 1.5 h; Cooling with ice-water bath;
参考文献
Ma, Huaibo; Petersen, Jeffrey L.; Young, Victor G.; Yee, Gordon T.; Jensen, Michael P.
Journal of the American Chemical Society, 2011 , vol. 133, # 15 p. 5644 - 5647
反应条件
sodium hydroxide in methanol 3 h; Ambient temperature;
参考文献
Kojima, Hideo; Nakamura, Keiichi; Yamamoto, Kazuhiko; Inoue, Hiroo
Synthesis, 1996 , # 10 p. 1193 - 1195
反应条件
sodium amalgam in tetrahydrofuran 2 h;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 2747 - 2756
反应条件
in water byproducts: NaCl; ZnCl2, the thiocarbamate in water, immediately pptn.; filtered hot to remove NaCl and any excess of unreacted thiocarbamate, dried (vac. at 80°C);
参考文献
Frigerio, A.; Halac, B.; Perec, M.
Inorganica Chimica Acta, 1989 , vol. 164, p. 149 - 154
反应条件
in methanol; dichloromethane T=20°C; 20 h;
参考文献
Gueguen; Boisde; Queffelec; Haelters; Thouvenot; Corbel; Nodet
Journal of Agricultural and Food Chemistry, 2000 , vol. 48, # 10 p. 4492 - 4499
参考文献
Alison,J.M.C.; Stephenson,T.A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1973 , p. 254 - 263
参考文献
Aubin, Lauren B.; Wagner, Tracy M.; Thoburn, John D.; Kesler, Brenda S.; Hutchison, Katherine A.; Schumaker, Robert R.; Parakka, James P.
Organic Letters, 2001 , vol. 3, # 21 p. 3413 - 3416
反应条件
in chloroform at room temp. for 2 h, concg.;
参考文献
Kupchik, E. J.; Calabretta, P. J.
Inorganic Chemistry, 1965 , vol. 4, p. 973 - 978