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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
127680-56-2
合成路线
（共 7 条）
127680-56-2
→
反应条件
93711-85-4
反应条件
1: Zn / tetrahydrofuran / Heating 2: acidic or basic hydrolyses with AG 50W-X2 ion exchange resin or aq. NaHCO3 3: imidazole View Scheme
参考文献
Ito, Yoshio; Kobayashi, Yuko; Terashima, Shiro
Tetrahedron Letters, 1989 , vol. 30, # 41 p. 5631 - 5634
127680-56-2
→
反应条件
76899-07-5
反应条件
1: 25 percent / 30percent H2O2, AcOH / H2O / 60 °C 2: 89 percent / imidazole / dimethylformamide / Ambient temperature View Scheme
参考文献
Kobayashi, Yuko; Ito, Yoshio; Terashima, Shiro
Tetrahedron, 1992 , vol. 48, # 1 p. 55 - 66
127680-56-2
→
反应条件
114341-89-8
反应条件
Multi-step reaction with 3 steps 1: 94 percent / Zn-dust / tetrahydrofuran / 0.03 h / Heating2: 89 percent / methanol / 4 h / Ambient temperature; ion-exchange-resin3: imidazole / dimethylformamide / Ambient temperature
参考文献
Kobayashi, Yuko; Ito, Yoshio; Terashima, Shiro Tetrahedron, 1992 , vol. 48, # 1 p. 55 - 66
127680-56-2
→
反应条件
114341-91-2
反应条件
Multi-step reaction with 2 steps 1: Zn / tetrahydrofuran / Heating2: acidic or basic hydrolyses with AG 50W-X2 ion exchange resin or aq. NaHCO3
参考文献
Ito, Yoshio; Kobayashi, Yuko; Terashima, Shiro Tetrahedron Letters, 1989 , vol. 30, # 41 p. 5631 - 5634
127680-56-2
→
反应条件
114341-94-5
反应条件
Multi-step reaction with 2 steps 1: 97 percent / Zn-dust / tetrahydrofuran / 0.03 h / Heating2: imidazole / dimethylformamide / Ambient temperature
参考文献
Kobayashi, Yuko; Ito, Yoshio; Terashima, Shiro Tetrahedron, 1992 , vol. 48, # 1 p. 55 - 66
127680-56-2
→
反应条件
114418-65-4
反应条件
Multi-step reaction with 2 steps 1: Zn / tetrahydrofuran / Heating2: acidic or basic hydrolyses with AG 50W-X2 ion exchange resin or aq. NaHCO3
参考文献
Ito, Yoshio; Kobayashi, Yuko; Terashima, Shiro Tetrahedron Letters, 1989 , vol. 30, # 41 p. 5631 - 5634
127680-54-0
→
反应条件
127680-56-2
反应条件
Multi-step reaction with 2 steps 1: 100 percent / H2 / 20percent Pd(OH)2/C / ethanol / 2 h / 760 Torr / Ambient temperature2: CaCO3 / benzene / 4 h / 80 °C
参考文献
Kobayashi, Yuko; Ito, Yoshio; Terashima, Shiro Tetrahedron, 1992 , vol. 48, # 1 p. 55 - 66
