5,5-二甲-2-(3'-甲酰基丙基)-1,3-二噁烷合成路线 （共 4 条）
反应条件
Collins oxidation agent in dichloromethane T=15°C; 0.333333 h;
参考文献
Deslongchamps; Belanger; Berney; Borschberg; Brousseau; Doutheau; Durand; Katayama; Lapalme; Leturc; Liao; MacLachlan; Maffrand; Marazza; Martino; Moreau; Ruest; Saint-Laurent; Saintonge; et al.
Canadian Journal of Chemistry, 1990 , vol. 68, # 1 p. 127 - 152
反应条件
1: p-toluenesulfonic acid / toluene / 24 h / Heating 2: 60 percent / Collins reagent (from chromic oxide, pyridine) / CH2Cl2 / 0.33 h / 15 °C View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 68, # 1 p. 127 - 152
反应条件
1: 90 percent / lithium aluminium hydride / diethyl ether / 12 h / Heating 2: 60 percent / Collins reagent (from chromic oxide, pyridine) / CH2Cl2 / 0.33 h / 15 °C View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 68, # 1 p. 127 - 152
反应条件
1: p-toluenesulfonic acid / toluene / 24 h / Heating 2: 60 percent / Collins reagent (from chromic oxide, pyridine) / CH2Cl2 / 0.33 h / 15 °C View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 68, # 1 p. 127 - 152
