反应条件
thionyl chloride in pentane CpFeC5H4COOH suspended in degassed n-pentane under Ar, treated at room temp. under vigorous stirring slowly with freshly purified SOCl2, heatedunder reflux, cooled; decanted, concd. in vac., decanted again, abs. olefin-free n-hexane added, concd. in vac., kept at -20°C for 24 h, ppt. filtered at -15°C, dried in Ar stream;
参考文献
Schmitt, Guenter; Klein, Peter; Ebertz, Wolfgang
Journal of Organometallic Chemistry, 1982 , vol. 234, # 1 p. 63 - 72