in benzene in boiling benzene, >6 h; (Ni(C5H5)2) and ((C5H5Ni)3((CO)2) come from thermal decompn. of ((C5H5NiCO)2); evapn. in vac.; extn. with CH2Cl2/hexane; concg. and cooling;
参考文献
Journal of Organometallic Chemistry, , vol. 56, p. 327 - 333
in benzene byproducts: (C5H5Ni)3(CO)2; in boiling benzene, >6 h; (Ni(C5H5)2) and (C5H5Ni)3(CO)2 come from thermal decompn. of ((C5H5NiCO)2); evapn. in vac.; extn. with CH2Cl2/hexane; concg. and cooling;
参考文献
Journal of Organometallic Chemistry, , vol. 56, p. 327 - 333
