反应条件
in ethylene glycol dimethyl ether byproducts: TlCl; under N2 or vac., to TiCl2(C6H12O2) in DME at 25°C CpTl added with stirring, 15 h, evapd., filtered, filtrate taken to dryness, extracted with toluene, filtered, washed with hexane, dried, refluxed in benzenefor 5 h; benzene removed;
参考文献
Marsella, John A.; Moloy, Kenneth G.; Caulton, Kenneth G.
Journal of Organometallic Chemistry, 1980 , vol. 201, # 2 p. 389 - 398
