2-(乙酰氧基甲基)-4-碘乙酸丁酯合成路线 （共 10 条）
反应条件
samarium; iodine in acetonitrile T=20°C; 48 h;
参考文献
RECORDATI S.A.
Patent: WO2004/7418 A1, 2004 ;
Location in patent: Page 12; 13 ;
反应条件
samarium; iodine in acetonitrile T=20°C; 48 h;
参考文献
RECORDATI S.A.
Patent: WO2004/7418 A1, 2004 ;
Location in patent: Page 13 ;
反应条件
1: 94 percent / pyridine, 4-dimethylaminopyridine (DMAP) / CH2Cl2 / 1 h / 0 °C 2: H2 / 10percent Pd/C / ethanol / 18 h / Ambient temperature 3: Et3N / CH2Cl2 / 1 h / -5 °C 4: NaI / acetone / 2 h / Heating View Scheme
参考文献
Geen; Grinter; Kincey; Jarvest
Tetrahedron, 1990 , vol. 46, # 19 p. 6903 - 6914
反应条件
1: H2 / 10percent Pd/C / ethanol / 18 h / Ambient temperature 2: Et3N / CH2Cl2 / 1 h / -5 °C 3: NaI / acetone / 2 h / Heating View Scheme
参考文献
Geen; Grinter; Kincey; Jarvest
Tetrahedron, 1990 , vol. 46, # 19 p. 6903 - 6914
反应条件
sodium iodide in acetone 2 h; Heating; Yield given;
参考文献
Geen; Grinter; Kincey; Jarvest
Tetrahedron, 1990 , vol. 46, # 19 p. 6903 - 6914
反应条件
1: Et3N / CH2Cl2 / 1 h / -5 °C 2: NaI / acetone / 2 h / Heating View Scheme
参考文献
Geen; Grinter; Kincey; Jarvest
Tetrahedron, 1990 , vol. 46, # 19 p. 6903 - 6914
反应条件
sodium iodide in acetonitrile 48 h; Ambient temperature;
参考文献
Mimero; Saluzzo; Amouroux
Synthetic Communications, 1995 , vol. 25, # 5 p. 613 - 627
反应条件
sodium iodide in acetonitrile 24 h; Ambient temperature;
参考文献
Mimero; Saluzzo; Amouroux
Synthetic Communications, 1995 , vol. 25, # 5 p. 613 - 627
反应条件
potassium carbonate in N,N-dimethyl-formamide 18 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 46, # 19 p. 6903 - 6914
反应条件
potassium carbonate in N,N-dimethyl-formamide 18 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 46, # 19 p. 6903 - 6914
