双(2-氯乙基)氨基磷酰二氯合成路线 (共 51 条)
反应条件
in tetrahydrofuran T=20 - 55°C;
参考文献
Chen, Xiaolan; Zhou, Yadong; Qu, Lingbo; Liu, Xiangqian; Yuan, Jinwei; Zhao, Yufen
Synthetic Communications, 2010 , vol. 40, # 13 p. 1992 - 1997
反应条件
in tetrahydrofuran T=20 - 55°C;
参考文献
Chen, Xiaolan; Zhou, Yadong; Qu, Lingbo; Liu, Xiangqian; Yuan, Jinwei; Zhao, Yufen
Synthetic Communications, 2010 , vol. 40, # 13 p. 1992 - 1997
反应条件
(i) Et2O, dibenzo-18-crown-6, (ii) NH3, benzene; Multistep reaction;
参考文献
Chiu,F.-T. et al.
Journal of Medicinal Chemistry, 1979 , vol. 22, p. 802 - 807
反应条件
(i) Et3N, benzene, (ii) NH3; Multistep reaction;
参考文献
Chiu,F.-T. et al.
Journal of Medicinal Chemistry, 1979 , vol. 22, p. 802 - 807
反应条件
(i) NaH, benzene, (ii) /BRN= 1072737/, (iii) /BRN= 4167662/; Multistep reaction;
参考文献
Chiu,F.-T. et al.
Journal of Medicinal Chemistry, 1979 , vol. 22, p. 802 - 807
参考文献
Dominguez, Maria J.; Sanmartin, Carmen; Font, Maria; Palop, Juan A.; San Francisco, Sara; Urrutia, Oscar; Houdusse, Fabrice; Garcia-Mina, Jose M.
Journal of Agricultural and Food Chemistry, 2008 , vol. 56, # 10 p. 3721 - 3731
反应条件
triethylamine in 1,4-dioxane
参考文献
Foster
Journal of Pharmaceutical Sciences, 1978 , vol. 67, # 5 p. 709 - 710
反应条件
triethylamine in tetrahydrofuran
参考文献
Foster
Journal of Pharmaceutical Sciences, 1978 , vol. 67, # 5 p. 709 - 710
反应条件
triethylamine in ethyl acetate
72 h; Yield given. Yields of byproduct given;
参考文献
Boyd, Victoria L.; Zon, Gerald; Himes, Vicky L.; Stalick, Judith K.; Mighell, Alan D.; Secor, Henry V.
Journal of Medicinal Chemistry, 1980 , vol. 23, # 4 p. 372 - 375
反应条件
dibenzo-18-crown-6 in benzene
T=25°C;
参考文献
Chiu; Chang; Ozkan; Zon; Fichter; Phillips
Journal of Pharmaceutical Sciences, 1982 , vol. 71, # 5 p. 542 - 551