反应条件
water; ammonium chloride in hexane
byproducts: Me2NLi, Et3GeH; in sealed evacuated ampule; in the course of 0.5 h at -20°C amide added to soln. of Et3GeLi; stirred at this temp. for 1.5 h; mixt. brought to room temp. and hydrolized with satd. NH4Cl soln.; products isolated by fractionation of the dried org. part ; GLC; mass-spectrometry; elem. anal.;
参考文献
Bravo-Zhivotovskii, D. A.; Pigarev, S. D.; Kalikhman, I. D.; Vyazankina, O. A.; Vyazankin, N. S.
Journal of Organometallic Chemistry, 1983 , vol. 248, # 1 p. 51 - 60