(吡啶鎓-1-基甲基)三氟硼酸盐合成路线 （共 10 条）
反应条件
in tetrahydrofuran; tert-butyl alcohol T=80°C; 2 h; Inert atmosphere;
参考文献
Raushel, Jessica; Sandrock, Deidre L.; Josyula, Kanth V.; Pakyz, Deborah; Molander, Gary A.
Journal of Organic Chemistry, 2011 , vol. 76, # 8 p. 2762 - 2769
反应条件
potassium phosphate; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water; tert-butyl alcohol T=110°C; Csp2-Csp3 Suzuki-Miyaura cross-coupling; 18 h; Inert atmosphereSealed tube;
参考文献
Molander, Gary A.; Beaumard, Floriane
Organic Letters, 2011 , vol. 13, # 5 p. 1242 - 1245
反应条件
palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; water T=80°C; Suzuki-Miyaura coupling; 45 h;
参考文献
Raushel, Jessica; Sandrock, Deidre L.; Josyula, Kanth V.; Pakyz, Deborah; Molander, Gary A.
Journal of Organic Chemistry, 2011 , vol. 76, # 8 p. 2762 - 2769
反应条件
palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; water T=80°C; Suzuki-Miyaura coupling; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 76, # 8 p. 2762 - 2769
反应条件
palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; water Suzuki-Miyaura coupling; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 76, # 8 p. 2762 - 2769
反应条件
palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; water Suzuki-Miyaura coupling; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 76, # 8 p. 2762 - 2769
反应条件
potassium phosphate; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water; tert-butyl alcohol
T=110°C; Csp2-Csp3 Suzuki-Miyaura cross-coupling; 1 h; Inert atmosphereSealed tube;
参考文献
Molander, Gary A.; Beaumard, Floriane
Organic Letters, 2011 , vol. 13, # 5 p. 1242 - 1245
反应条件
potassium phosphate; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water; tert-butyl alcohol
T=110°C; Csp2-Csp3 Suzuki-Miyaura cross-coupling; 4 h; Inert atmosphereSealed tube;
参考文献
Molander, Gary A.; Beaumard, Floriane
Organic Letters, 2011 , vol. 13, # 5 p. 1242 - 1245
反应条件
palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; water
T=80°C; Suzuki-Miyaura coupling; 45 h;
参考文献
Raushel, Jessica; Sandrock, Deidre L.; Josyula, Kanth V.; Pakyz, Deborah; Molander, Gary A.
Journal of Organic Chemistry, 2011 , vol. 76, # 8 p. 2762 - 2769
反应条件
1: With potassium phosphate; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water; tert-butyl alcohol
T=110°C; Csp2-Csp3 Suzuki-Miyaura cross-coupling; Inert atmosphereSealed tube;
2: With hydrogenchloride in diethyl ether
参考文献
Molander, Gary A.; Beaumard, Floriane
Organic Letters, 2011 , vol. 13, # 5 p. 1242 - 1245
