3-(3-甲氧基苯基)苯甲醛合成路线 （共 6 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethanol; toluene Suzuki cross-coupling; 1 h; Heating;
参考文献
Journal of Medicinal Chemistry, , vol. 47, # 21 p. 4998 - 5008
反应条件
potassium fluoride; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide T=100°C; 15 h;
参考文献
Chemistry Letters, , p. 1711 - 1714
Tetrahedron, , vol. 50, # 28 p. 8301 - 8316
反应条件
1: pyridinium chlorochromate / CH2Cl2 2: 83 percent / KF / (η3-C3H5PdCl)2 / dimethylformamide / 15 h / 100 °C View Scheme
参考文献
Tetrahedron, , vol. 50, # 28 p. 8301 - 8316
反应条件
1: SbF3 2: 83 percent / KF / (η3-C3H5PdCl)2 / dimethylformamide / 15 h / 100 °C View Scheme
参考文献
Chemistry Letters, , p. 1711 - 1714
反应条件
hydrogenchloride; sodium; sodium carbonate; Merrifield resin; tetrakis(triphenylphosphine) palladium(0) 2.) DME, reflux, 24 h; 3.) dioxan, 80 deg C, 48 h; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 39, # 24 p. 4179 - 4182
反应条件
sodium tetrahydroborate in methanol
2 h;
参考文献
ASTRAZENECA AB; ASTEX THERAPEUTICS
Patent: WO2006/65204 A1, 2006 ;
Location in patent: Page/Page column 150 ;
WO 2006/065204 A1
