反应条件
in diethyl ether; hexane Ar-atmosphere; treatment of Zr-complex (in Et2O) with slight excess of LiMe (in hexane) at -30°C, slow warming to room temp., stirring for 12 h; removal of volatiles, extn. into light petroleum, filtration, solvent removal (reduced pressure); product mixt. (1:1) not sepd., detd. by (1)H-NMR spectroscopy;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , # 2 p. 217 - 226
