反应条件
in diethyl ether inert atm., Schlenk technique; dropwise addn. of thienyl-Li in ether to Zr-complex in ether (-78°C), warmed to room temp. over 12 h; evapn., extn. (CHCl3), filtration, evapn. (red oily residue), washed (pentane), evapn., not further separated; elem. anal.;
参考文献
Organometallics, , vol. 11, p. 1646 - 1655
