(S)-3-甲基-2-((苯氧基羰基)氨基)丁酸合成路线 (共 18 条)
反应条件
sodium hydroxide; potassium hydrogencarbonate 1.5 h; Ambient temperature;
参考文献
Wuts, Peter G. M.; Pruitt, Lynn E.
Synthesis, 1989 , # 8 p. 622 - 623
反应条件
lithium hydroxide; sulfuric acid; lithium chloride in n-heptane; water; toluene
反应条件
lithium hydroxide; sulfuric acid; lithium carbonate in n-heptane; water; toluene
反应条件
1: 2-aminoisovaleric acid With tetra(n-butyl)ammonium hydroxide in methanol T=20°C; 1 h; 2: carbonic acid diphenyl ester in acetonitrile T=20°C; 3.166 h;
参考文献
Yamada, Shuhei; Koga, Koichi; Sudo, Atsushi; Goto, Mitsuaki; Endo, Takeshi
Journal of Polymer Science, Part A: Polymer Chemistry, 2013 , vol. 51, # 17 p. 3726 - 3731
反应条件
1: 94 percent / BH3*THF / tetrahydrofuran / 3 h / 0 °C 2: t-BuOK / tetrahydrofuran / 1 h / 0 °C View Scheme
参考文献
Wuts, Peter G. M.; Pruitt, Lynn E.
Synthesis, 1989 , # 8 p. 622 - 623
反应条件
NaH in tetrahydrofuran; water; toluene
参考文献
Abbott Laboratories
Patent: US6160122 A1, 2000 ;
反应条件
sodium hydroxide in tetrahydrofuran; n-heptane; water; toluene
参考文献
Abbott Laboratories
Patent: US6160122 A1, 2000 ;
反应条件
hydrogenchloride in tetrahydrofuran; water; toluene
参考文献
Abbott Laboratories
Patent: US6160122 A1, 2000 ;
反应条件
hydrogenchloride; NaH in tetrahydrofuran; water; toluene
参考文献
Abbott Laboratories
Patent: US6160122 A1, 2000 ;
反应条件
in tetrahydrofuran; n-heptane; water; toluene
参考文献
Abbott Laboratories
Patent: US6160122 A1, 2000 ;