2-氯-1.3-丁二烯合成路线 (共 128 条)
反应条件
bis (3-tert-butyl-4-hydroxy-5-methyl phenyl)-sulfide in toluene T=50°C; 16 h; Further byproducts given;
参考文献
Klaerner, Frank-Gerrit; Krawczyk, Bernd; Ruster, Volker; Deiters, Ulrich K.
Journal of the American Chemical Society, 1994 , vol. 116, # 17 p. 7646 - 7657
参考文献
Stewart,C.A.
Journal of the American Chemical Society, 1971 , vol. 93, # 19 p. 4815 - 4821
反应条件
(i) Mg, (ii) CuCl2; Multistep reaction;
参考文献
Heinrich,F.; Luettke,W.
Justus Liebigs Annalen der Chemie, 1978 , p. 1880 - 1886
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform-d1; water-d2 T=20°C; 140 h; Product distribution;
参考文献
Cottrell; Golding; Munter; Watson
Chemical Research in Toxicology, 2001 , vol. 14, # 11 p. 1552 - 1562
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=20°C; 48 h; Product distribution;
参考文献
Cottrell; Golding; Munter; Watson
Chemical Research in Toxicology, 2001 , vol. 14, # 11 p. 1552 - 1562
反应条件
tert-butyl-pyrocatechol; chlorine in tetrachloromethane T=-5 - 0°C; Further byproducts given. Yields of byproduct given;
参考文献
Mkryan, G. M.; Airapetyan, R. Kh.; Mkryan, G. G.; Kaplanyan, E. E.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 1242 - 1247
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 7 p. 1387 - 1393
反应条件
tert-butyl-pyrocatechol; chlorine in tetrachloromethane T=-5 - 0°C; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mkryan, G. M.; Airapetyan, R. Kh.; Mkryan, G. G.; Kaplanyan, E. E.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 1242 - 1247
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 7 p. 1387 - 1393
参考文献
Petrov,A.A.; Babayan,V.O.
J. Gen. Chem. USSR (Engl. Transl.), 1964 , vol. 34, # 8 p. 2633 - 2638,2654 - 2658
参考文献
Petrow
Zhurnal Obshchei Khimii, 1952 , vol. 22, p. 1516,1519,1523;engl.Ausg.S.1557,1558,1562
Doklady Akademii Nauk SSSR, 1951 , vol. 78, p. 63,64
Chem.Abstr., 1952 , p. 881
参考文献
Carothers; Berchet
Journal of the American Chemical Society, 1933 , vol. 55, p. 1629
Full Text Show Details
Petrow
Zhurnal Obshchei Khimii, 1943 , vol. 13, p. 111
Zhurnal Obshchei Khimii, 1949 , vol. 19, p. 1050
Chem.Abstr., 1944 , p. 330,1950 1003