sodium hydroxide; tellurium; hydroxymethanesulfinic acid sodium salt in tetrahydrofuran; water T=50 - 55°C; 3 h; Title compound not separated from byproducts;
参考文献
Kumar, Archana; Dittmer, Donald C.
Tetrahedron Letters, 1994 , vol. 35, # 31 p. 5583 - 5586
1H-imidazole; 2,6-dimethylpyridine; water; iodine; triphenylphosphine in 1,2-dichloro-ethane; benzene T=75 - 80°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
1H-imidazole; 2,6-dimethylpyridine; water; iodine; triphenylphosphine in 1,2-dichloro-ethane; benzene T=75 - 80°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
