5,5-二甲基-1,3-环己二酮合成路线 (共 504 条)
反应条件
12-tungestocobaltic acid supported on nano silica T=80°C; 0.05 h; neat (no solvent);
参考文献
Rafiee, Ezzat; Khodayari, Maryam; Kahrizi, Masoud; Tayebee, Reza
Journal of Molecular Catalysis A: Chemical, 2012 , vol. 358, p. 121 - 128
反应条件
in chloroform Ambient temperatureovernight;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 17, p. 777
Zhurnal Organicheskoi Khimii, , vol. 17, # 4 p. 883 - 884
反应条件
manganese triacetate in acetic acid 0.05 h; Heating;
参考文献
Heterocycles, , vol. 54, # 1 p. 171 - 183
反应条件
bis(succinimide) sulfide in 1,2-dichloro-ethane T=20 - 25°C; 1 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 22, p. 86 - 92
Zhurnal Organicheskoi Khimii, , vol. 22, # 1 p. 100 - 106
反应条件
hydrogenchloride; amalgamated zinc
参考文献
Dey; Linstead
Journal of the Chemical Society, 1935 , p. 1063
反应条件
1: pyridine / CH2Cl2 2: dimethylformamide / 24 h / 20 °C View Scheme
参考文献
Gopalsamy, Ariamala; Yang, Hui; Ellingboe, John W.; Kees, Kenneth L.; Yoon, Jeanne; Murrills, Richard
Bioorganic and Medicinal Chemistry Letters, 2000 , vol. 10, # 15 p. 1715 - 1718
反应条件
T=20°C; Solid phase reaction; condensation; 0.5 h;
参考文献
Kaupp, Gerd; Schmeyers, Jens; Boy, Juergen
Advanced Synthesis and Catalysis, 2000 , vol. 342, # 3 p. 269 - 280
反应条件
1: 82 percent / toluene / 24 h / 20 °C 2: 30 percent / acetic acid / 10 h / Heating View Scheme
参考文献
Vovk; Sukach; Chubaruk; Chernega; Bol'but
Russian Journal of Organic Chemistry, 2007 , vol. 43, # 2 p. 256 - 262
反应条件
1: (i) NaOMe, MeOH, (ii) /BRN= 969135/ 2: Py / benzene 3: Et3N, PhCO2H / xylene View Scheme
参考文献
Heathcock,C.H.; Gray,D.
Tetrahedron, 1971 , vol. 27, p. 1239 - 1246
反应条件
1: NH3 2: Py / 1,2-dimethoxy-ethane View Scheme
参考文献
Foster, James E.; Nicholson, Jesse M.; Butcher, Raymond; Stables, James P.; Edafiogho, Ivan O.; Goodwin, Angela M.; Henson, Michael C.; Smith, Carlynn A.; Scott
Bioorganic and Medicinal Chemistry, 1999 , vol. 7, # 11 p. 2415 - 2425