2,2-二甲基-1,3-丙二醇合成路线 (共 467 条)
反应条件
1: triphenylbismuthine With boron trichloride in dichloromethane T=-78°C; 4 h; 2: With methanol T=20°C; 0.5 h; 3: 3-hydroxy-2,2-dimethylpropanol in methanol T=20°C; 1 h;
参考文献
Yasuike, Shuji; Nakata, Kazuhide; Qin, Weiwei; Kaji, Toshiyuki; Kurita, Jyoji
Chemistry Letters, 2006 , vol. 35, # 12 p. 1402 - 1403
反应条件
water; phosphorus trichoride in toluene T=35 - 110°C;
参考文献
DOW GLOBAL TECHNOLOGIES INC.; WORKU, Anteneh; BHARADWAJ, Ashwin; THIBAULT, Raymond; WILSON, Mark; POTTS, Douglas
Patent: WO2010/25165 A1, 2010 ;
Location in patent: Page/Page column 28 ;
反应条件
in tetrahydrofuran T=70°C; 2 h; Inert atmosphere;
参考文献
Gosset, Gaelle; Clement, Jean-Louis; Culcasi, Marcel; Rockenbauer, Antal; Pietri, Sylvia
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 7 p. 2218 - 2230
反应条件
hydrogenchloride; anhydrous phosphorus trichloride; mercury in water
参考文献
MONSANTO COMPANY
Patent: EP594553 A1, 1994 ;
反应条件
T=130 - 140°C; P=150 Torr; 4 h;
参考文献
Maffei, Michel; Buono, Gerard
Tetrahedron, 2003 , vol. 59, # 44 p. 8821 - 8825
反应条件
nitric acid in water
参考文献
Evans, Andrew R.; Martin, Russell; Taylor, Giles A.; Yap, C. H. Maurice
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1635 - 1640
参考文献
Just
Monatshefte fuer Chemie, 1896 , vol. 17, p. 79
参考文献
Grachev; Charaev; Kurochkina; Batalova; Soboleva; Vasyanina; Nifant'ev
Russian Journal of General Chemistry, 2011 , vol. 81, # 10 p. 2129 - 2135
反应条件
1: With titanium(IV) isopropylate T=220°C; 8 h; 2: With sodium hydroxide in water Product distribution / selectivity;
参考文献
Kim, Hyunkyu; Lee, Kyeseok; Lee, Kyu Il; Chun, Byoungkue
Patent: US2007/15933 A1, 2007 ;
Location in patent: Page/Page column 6 ;
参考文献
Eastman Kodak Co.
Patent: US2743187 , 1952 ;