2,2-二甲基-1,3-丙二醇合成路线 （共 467 条）
反应条件
pyridine; phosphorus tribromide in diethyl ether
参考文献
White,D.W. et al.
Journal of the American Chemical Society, 1970 , vol. 92, p. 7125 - 7135
反应条件
in benzene 36 h; Heating;
参考文献
Barton, Derek H. R.; Finet, Jean-Pierre; Motherwell, William B.; Pichon, Clotilde
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry, 1987 , p. 251 - 259
反应条件
1: 91 percent / CH2Cl2 / 4 h / 60 °C / Irradiation View Scheme
参考文献
Barton, Derek H. R.; Finet, Jean-Pierre; Pichon, Clotilde
Journal of the Chemical Society, Chemical Communications, 1986 , # 1 p. 65 - 66
反应条件
toluene-4-sulfonic acid in phosphorus tribromide; 1,2-dichloro-ethane
参考文献
Bartels; Gunter
Patent: US4847391 A1, 1989 ;
反应条件
toluene-4-sulfonic acid in benzene 72 h; Reflux;
参考文献
Bringmann, Sebastian; Ahmed, Saleh A.; Hartmann, Ramona; Mattay, Jochen
Synthesis, 2011 , # 14 art. no. T36111SS, p. 2291 - 2296
反应条件
toluene-4-sulfonic acid in benzene acetalation; 24 h; Heating;
参考文献
Eckert, Jean-Francois; Nicoud, Jean-Francois; Nierengarten, Jean-Francois; Liu, Sheng-Gao; Echegoyen, Luis; Barigelletti, Francesco; Armaroli, Nicola; Ouali, Lahoussine; Krasnikov, Victor; Hadziioannou, Georges
Journal of the American Chemical Society, 2000 , vol. 122, # 31 p. 7467 - 7479
反应条件
toluene-4-sulfonic acid in hexane; dichloromethane
参考文献
Schering Aktiengesellschaft
Patent: US5089635 A1, 1992 ;
反应条件
(NH4)2S2O8; silver nitrate; trifluoroacetic acid in water T=35 - 80°C; 0.133333 h;
参考文献
Hackler, Ronald E.; Dreikorn, Barry A.; Johnson, George W.; Varie, David L.
Journal of Organic Chemistry, 1988 , vol. 53, # 24 p. 5704 - 5709
反应条件
(NH4)2S2O8; sulfuric acid in water T=100°C; 2 h; Yields of byproduct given;
参考文献
Hackler, Ronald E.; Dreikorn, Barry A.; Johnson, George W.; Varie, David L.
Journal of Organic Chemistry, 1988 , vol. 53, # 24 p. 5704 - 5709
反应条件
toluene-4-sulfonic acid in dichloromethane T=20°C; 18 h;
参考文献
Schwede, Wolfgang; Moeller, Carsten; Schmidt, Anja; Fuhrmann, Ulrike; Rotgeri, Andrea; Kirkland, Thomas Andrew; Wyrwa, Ralf
Patent: US2009/75989 A1, 2009 ;
Location in patent: Page/Page column 69 ;
US 20090075989 A1
