2,2-二甲基-1,3-丙二醇合成路线 （共 467 条）
反应条件
triethylamine; trichlorophosphate in dichloromethane
T=0°C; 0.5 h;
参考文献
Yamada, Takeshi; Takemura, Kazunobu; Yoshida, Jun-Ichi; Yamago, Shigeru
Angewandte Chemie - International Edition, 2006 , vol. 45, # 45 p. 7575 - 7578
反应条件
trichlorophosphate in toluene
T=50 - 75°C; 2 h;
参考文献
DAIHACHI CHEMICAL INDUSTRY CO., LTD.
Patent: EP1808437 A1, 2007 ;
Location in patent: Page/Page column 13-14; 17 ;
反应条件
1: tetraphosphorus decasulfide / toluene
2: potassium iodide; iodine / water
View Scheme
参考文献
Lach, Slawomir; Demkowicz, Sebastian; Witt, Dariusz
Tetrahedron Letters, 2013 , vol. 54, # 51 p. 7021 - 7023
反应条件
(i) P2S5, (ii) /BRN= 605310/; Multistep reaction;
参考文献
Pudovik,A.N. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1972 , vol. 42, p. 2638 - 2642,2629 - 2632
反应条件
selenium(IV) oxide in cyclohexane
Heating;
参考文献
Kluefers, Peter; Reichvilser, Moritz M.
European Journal of Inorganic Chemistry, 2008 , # 3 p. 384 - 396
反应条件
in ethyl acetate; toluene
参考文献
Sandoz Ltd., (Sandoz AG)
Patent: US3948946 A1, 1976 ;
参考文献
Apel; Tollens
Justus Liebigs Annalen der Chemie, 1896 , vol. 289, p. 38
Chemische Berichte, 1894 , vol. 27, p. 1088
