2,2-二甲基-1,3-丙二醇合成路线 (共 467 条)
反应条件
1: Et3N
2: Dess-Martin periodinane
View Scheme
参考文献
Angle, Steven R.; Bernier, Daniel S.; El-Said, Nahla A.; Jones, Darin E.; Shaw, Stephanie Z.
Tetrahedron Letters, 1998 , vol. 39, # 23 p. 3919 - 3922
反应条件
cesium fluoride in tert-butyl alcohol
参考文献
Ogilvie,K.K. et al.
Journal of the American Chemical Society, 1977 , vol. 99, p. 1277 - 1278
反应条件
p-toluenesulfonic acid monohydrate in n-heptane; water
参考文献
BASF Aktiengesellschaft
Patent: US5344995 A1, 1994 ;
反应条件
Multistep reaction.;
参考文献
Kopp, Felix; Wunderlich, Stefan; Knochel, Paul
Chemical Communications, 2007 , # 20 p. 2075 - 2077
参考文献
McCormick,J.E.; McElhinney,R.S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976 , p. 2533 - 2540
反应条件
in tetrahydrofuran
0.666667 h; Dean-StarkReflux;
参考文献
Zhao, Yigang; Snieckus, Victor
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 7 p. 1527 - 1532
反应条件
polyacrylonitrile hybrid fiber mat supported solid acid catalyst in cyclohexane
Reflux;
参考文献
Shao, Linjun; Du, Yijun; Xing, Guiying; Lv, Weixi; Liang, Xuezheng; Qi, Chenze
Monatshefte fur Chemie, 2012 , vol. 143, # 8 p. 1199 - 1203
反应条件
sulfated zirconia in benzene
3.5 h; Heating;
参考文献
Bandgar, Babasaheb P.; Gaikwad, Nandkumar B.
Monatshefte fur Chemie, 1998 , vol. 129, # 6-7 p. 719 - 722
反应条件
indium trifluoromethanesulfonate
T=20°C; 0.5 h; Neat (no solvent);
参考文献
Smith, Brendan M.; Kubczyk, Tomasz M.; Graham, Andrew E.
Tetrahedron, 2012 , vol. 68, # 38 p. 7775 - 7781
反应条件
manganese(IV) oxide; In(OSO2CF3)3 in dichloromethane
T=20°C; 24 h;
参考文献
Smith, Brendan M.; Graham, Andrew E.
Tetrahedron Letters, 2007 , vol. 48, # 28 p. 4891 - 4894