2,2-二甲基-1,3-丙二醇合成路线 (共 467 条)
反应条件
tetraphosphorus decasulfide in benzene
T=50°C;
参考文献
Doszczak, Leszek; Rachon, Janusz
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 10 p. 1271 - 1279
反应条件
polyacrylonitrile hybrid fiber mat supported solid acid catalyst in cyclohexane
Reflux;
参考文献
Shao, Linjun; Du, Yijun; Xing, Guiying; Lv, Weixi; Liang, Xuezheng; Qi, Chenze
Monatshefte fur Chemie, 2012 , vol. 143, # 8 p. 1199 - 1203
反应条件
indium trifluoromethanesulfonate in dichloromethane
T=20°C; 0.5 h;
参考文献
Smith, Brendan M.; Kubczyk, Tomasz M.; Graham, Andrew E.
Tetrahedron, 2012 , vol. 68, # 38 p. 7775 - 7781
反应条件
indium trifluoromethanesulfonate
T=20°C; 0.5 h; Neat (no solvent);
参考文献
Smith, Brendan M.; Kubczyk, Tomasz M.; Graham, Andrew E.
Tetrahedron, 2012 , vol. 68, # 38 p. 7775 - 7781
反应条件
N-(4-methyoxybenzyl)-2-cyanopyridinium hexafluoroantimonate in toluene
1.5 h; Heating;
参考文献
Lee; Takata; Endo
Synthesis, 1991 , # 5 p. 368 - 370
反应条件
1: 68 percent / toluene / 0.25 h
2: 60 percent / para-toluenesulfonic acid / heptane / 1.5 h / 20 °C
View Scheme
参考文献
Gvozdik; Gal'chenko; Musavirov
Russian Journal of General Chemistry, 1996 , vol. 66, # 5 p. 784 - 787
反应条件
oxalic acid in toluene
48 h; Heating / reflux;
参考文献
INVISTA Technologies S.a.r.l.
Patent: EP1214282 B1, 2005 ;
Location in patent: Page/Page column 10 ;
反应条件
toluene-4-sulfonic acid in toluene
Condensation;
参考文献
Maslinska-Solich; Sowa; Czuba
Polish Journal of Chemistry, 1999 , vol. 73, # 8 p. 1339 - 1343
反应条件
toluene-4-sulfonic acid in toluene
2 h; RefluxInert atmosphere;
参考文献
Hadfield, Maximillian S.; Lee, Ai-Lan
Chemical Communications, 2011 , vol. 47, # 4 p. 1333 - 1335
反应条件
(NH4)2S2O8; sulfuric acid in water
T=100°C; 2 h; Yields of byproduct given;
参考文献
Hackler, Ronald E.; Dreikorn, Barry A.; Johnson, George W.; Varie, David L.
Journal of Organic Chemistry, 1988 , vol. 53, # 24 p. 5704 - 5709