2,2-二甲基-1,3-丙二醇合成路线 （共 467 条）
反应条件
sodium anschliessend mit Jodmethan;
参考文献
Brown; van Gulick
Journal of the American Chemical Society, 1955 , vol. 77, p. 1089,1091
反应条件
potassium hydroxide in tetrahydrofuran 0.5 h; Heating;
参考文献
Toivonen, Hannu
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1984 , vol. 38, # 1 p. 37 - 42
反应条件
sodium hydride 1.) THF, reflux, 1 h, 2.) THF, 23-90 deg C, 22 h; Yield given. Multistep reaction;
参考文献
Effenberger, Franz; Eichhorn, Joachim; Roos, Juergen
Tetrahedron: Asymmetry, 1995 , vol. 6, # 1 p. 271 - 282
反应条件
potassium hydroxide; sulfuric acid in water
参考文献
Dale, Johannes; Fredriksen, Siw B.
Acta Chemica Scandinavica, 1991 , vol. 45, # 1 p. 82 - 91
反应条件
Eintragen des Reaktionsgemisches in heisse wss.Natronlauge;
参考文献
Schmoyer; Case
Nature (London, United Kingdom), 1959 , vol. 183, p. 389
反应条件
1: 96 percent / pyridine 2: 71 percent / ethane-1,2-diol / 2 h / Heating 3: 85 percent / NaOH / H2O / 48 h / Heating View Scheme
参考文献
Brown,H.C. et al.
Journal of the American Chemical Society, 1977 , vol. 99, # 2 p. 505 - 509
反应条件
cyclohexanone; bis(cyclopentadienyl)zirconium dihydride T=150°C; 8 h;
参考文献
Nakano, Tatsuya; Terada, Takanobu; Ishii, Yasutaka; Ogawa, Masaya
Synthesis, 1986 , # 9 p. 774 - 776
反应条件
1 Au-Pd/TiO2; oxygen; sodium hydroxide T=80°C; P=2250.23 Torr; 4 h;
参考文献
Kotionova, Tatyana; Lee, Christopher; Miedziak, Peter J.; Dummer, Nicholas F.; Willock, David J.; Carley, Albert F.; Morgan, David J.; Knight, David W.; Taylor, Stuart H.; Hutchings, Graham J.
Catalysis Letters, 2012 , vol. 142, # 9 p. 1114 - 1120
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethylsulfoxide-d6 T=23°C; product ratio was determined by 1H NMR; Product distribution;
参考文献
Corey; Palani, Anandan
Tetrahedron Letters, 1995 , vol. 36, # 44 p. 7945 - 7948
反应条件
1: SOCl2 / pyridine 2: K2Cr2O7, aq. H2SO4 / benzene View Scheme
参考文献
Kirmse,W. et al.
Chemische Berichte, 1966 , vol. 99, p. 2579 - 2592
