(3beta,5alpha)-胆甾烷-3-基乙酸酯合成路线 （共 13 条）
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide; diethyl ether; tert-butyl alcohol
参考文献
Bose, Ajay K.; Mangiaracina, Pietro
Tetrahedron Letters, 1987 , vol. 28, # 22 p. 2503 - 2506
反应条件
18-crown-6 ether; tert-butylamine in diethyl ether further solvent;
参考文献
Barrett, Anthony G. M.; Godfrey, Christopher R. A.; Hollinshead, David M.; Prokopiou, Panayiotis A.; Barton, Derek H. R.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1501 - 1509
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide; water 2.5 h; Irradiation; Yield given;
参考文献
Portella, C.; Deshayes, H.; Pete, J. P.; Scholler, D.
Tetrahedron, 1984 , vol. 40, # 19 p. 3635 - 3644
反应条件
chromium(VI) oxide; acetic acid T=95°C; Erhitzen des aus dem Reaktionsgem. mit Hilfe von Semicarbazid isolierten 3β-Acetoxy-5α-androstanon-(17)-semicarbazons mit einem Gemisch von Essigsaeure und konz.wss.Salzsaeure und Erhitzen des Reaktionsprod. mit aethanol.KOH;
参考文献
Ruzicka et al.
Helvetica Chimica Acta, 1934 , vol. 17, p. 1407,1412
Full Text Show Details
Ruzicka; Goldberg; Bruengger
Helvetica Chimica Acta, 1934 , vol. 17, p. 1389,1392
Full Text Show Details
Schering Corp.
Patent: US2232735 , 1935 ;
反应条件
sodium; sodium amide in N,N,N',N',N'',N''-hexamethylphosphoric triamide; diethyl ether 0.5 h;
参考文献
Canadian Journal of Chemistry, , vol. 62, p. 2063 - 2072
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide; diethyl ether
参考文献
Canadian Journal of Chemistry, , vol. 62, p. 2063 - 2072
反应条件
lipase from Candida cylindracea; octanol in various solvent(s) T=37°C; 144 h;
参考文献
Tetrahedron Letters, , vol. 28, # 52 p. 6549-6552
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide; diethyl ether; tert-butyl alcohol
参考文献
Canadian Journal of Chemistry, , vol. 62, p. 2063 - 2072
反应条件
18-crown-6 ether; tert-butylamine in diethyl ether further solvent;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1501 - 1509
反应条件
sodium; sodium amide in N,N,N',N',N'',N''-hexamethylphosphoric triamide; diethyl ether 0.5 h;
参考文献
Deshayes, Henri; Pete, Jean-Pierre
Canadian Journal of Chemistry, 1984 , vol. 62, p. 2063 - 2072
