(4-甲氧羰基苄基)三苯基溴化膦合成路线 （共 8 条）
反应条件
in acetonitrile Reflux;
参考文献
Motoshima, Kazunori; Ishikawa, Minoru; Hashimoto, Yuichi; Sugita, Kazuyuki
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 10 p. 3156 - 3172
反应条件
1: 77 percent / NBS; benzoyl peroxide / CCl4 / 3 h / 100 °C 2: 75 percent / toluene / 5 h / 120 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 8, # 6 p. 1479 - 1487
反应条件
bromine 1.) CCl4, irradiation; 2.) benzene; Yield given. Multistep reaction;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 94, # 3 p. 215 - 232
反应条件
1.1: KOt-Bu / tetrahydrofuran / 1 h / 80 °C 1.2: tetrahydrofuran / 0.5 h / 80 °C 2.1: H2 / 5percent Pd/C / ethanol; ethyl acetate / 0.67 h / 20 °C / 1875.19 Torr 3.1: aq. NaOH / methanol / 15 h / 20 °C View Scheme
参考文献
Shinkai; Ito; Iida; Kitao; Yamada; Uchida
Journal of Medicinal Chemistry, 2000 , vol. 43, # 24 p. 4667 - 4677
反应条件
1: 75 percent / DBU / tetrahydrofuran / 8 h 2: 100 percent / H2 / Pd/C / ethyl acetate / 6 h View Scheme
参考文献
Taylor, Edward C.; Dowling, James E.
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 4 p. 453 - 456
反应条件
potassium tert-butylate in toluene T=20°C; 1 h; Cooling with acetone-dry ice;
参考文献
Listvan, V. N.; Stasyuk, A. P.; Kurgan, L. N.
J. Gen. Chem. USSR (Engl. Transl.), 1987 , vol. 57, # 7 p. 1534 - 1540,1366 - 1371
反应条件
1: [[4-(methoxycarbonyl)phenyl]methyl]triphenyl-phosphonium bromide With 18-crown-6 ether; potassium carbonate in tetrahydrofuran; dichloromethane
0.0833333 h;
2: benzaldehyde in tetrahydrofuran; dichloromethane
10 h; Heating;
参考文献
Dogan, Zeynep; Paulini, Ralph; Stuetz, Jan A. Rojas; Narayanan, Sukunath; Richert, Clemens
Journal of the American Chemical Society, 2004 , vol. 126, # 15 p. 4762 - 4763
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
Hydrolysis; Wittig olefination; 8 h;
参考文献
Taylor, Edward C.; Dowling, James E.
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 4 p. 453 - 456
