2-[乙酰氧基(苯基)甲基]丙烯酸甲酯合成路线 (共 24 条)
反应条件
pyridine in dichloromethane T=0°C; 1 h;
参考文献
Annunziata, Rita; Benaglia, Maurizio; Cinquini, Mauro; Cozzi, Franco; Raimondi, Laura
Journal of Organic Chemistry, 1995 , vol. 60, # 15 p. 4697 - 4706
反应条件
montmorillonite K-10 T=40°C; 4 h;
参考文献
Das, Biswanath; Banerjee, Joydeep; Majhi, Anjoy; Chowdhury, Nikhil; Venkateswarlu, Katta; Holla, Harish
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 7 p. 1729 - 1733
反应条件
1: 1,4-diaza-bicyclo[2.2.2]octane / methanol / 168 h / 20 °C / Inert atmosphere 2: pyridine / dichloromethane / -20 - 20 °C / Inert atmosphere View Scheme
参考文献
Foucaud, Andre; Guemmout, Farid El
Bulletin de la Societe Chimique de France, 1989 , # 3 p. 403 - 408
反应条件
amberlyst-15 T=40°C; 2 h;
参考文献
Garrido, Narciso M.; Garcia, Mercedes; Sanchez, M. Rosa; Diez, David; Urones, Julio G.
Synlett, 2010 , # 3 art. no. D28909ST, p. 387 - 390
反应条件
Multistep reaction.;
参考文献
Sheng, Shou-Ri; Huang, Fang-Fang; Lin, Shu-Ying; Liu, Xiao-Ling; Huang, Xian
Synthesis, 2007 , # 9 p. 1373 - 1377
反应条件
triethylamine T=20°C; 0.25 h;
参考文献
Zhong, Weihui; Zhao, Yongzhi; Guo, Baoming; Wu, Peng; Su, Weike
Synthetic Communications, 2008 , vol. 38, # 19 p. 3291 - 3302
反应条件
tetrakis(triphenylphosphine) palladium(0); formic acid; triethylamine; triphenylphosphine in tetrahydrofuran Yield given. Yields of byproduct given;
参考文献
Pachamuthu, Kandaswamy; Vankar, Yashwant D.
Tetrahedron Letters, 1998 , vol. 39, # 30 p. 5439 - 5442
反应条件
1.1: methanol; ammonia / 1 h / 20 °C 2.1: iodine / chloroform / 0.08 h 2.2: 0.5 h / 20 °C View Scheme
参考文献
Batchu, Harikrishna; Bhattacharyya, Soumya; Batra, Sanjay
Organic Letters, 2012 , vol. 14, # 24 p. 6330 - 6333
反应条件
1.1: DABCO / tetrahydrofuran; H2O / 0.5 h 1.2: 87 percent / 18 h / 20 °C 2.1: 79 percent / polyphosphoric acid / 7 h / 80 - 90 °C 3.1: 93 percent / DBU / tetrahydrofuran / 1 h / 20 °C View Scheme
参考文献
Lee, Chang Gon; Lee, Ka Young; Lee, Sangku; Kim, Jae Nyoung
Tetrahedron, 2005 , vol. 61, # 6 p. 1493 - 1499
反应条件
triethylamine T=90°C; 2.5 h;
参考文献
Zhong, Weihui; Zhao, Yongzhi; Su, Weike
Tetrahedron, 2008 , vol. 64, # 23 p. 5491 - 5496