4,4',4''-三(N-3-甲基苯基-N-苯基氨基)三苯胺合成路线 (共 3 条)
反应条件
palladium diacetate; tri-tert-butyl phosphine; sodium t-butanolate in o-xylene T=120°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 39, # 16 p. 2367 - 2370
反应条件
potassium hydroxide; 2,5-Dihydroxy-5-methyl-3-morpholin-4-yl-cyclopent-2-enone; copper(I) bromide in para-menthadiene T=115 - 125°C; Ullmann Condensation; 6 h; Product distribution / selectivity;
参考文献
JP2005/350416 A, ;
Page/Page column 41-42 ;
反应条件
1: 51 percent / mercuric oxide; I2 / ethanol / 4 h / 78 °C 2: 75 percent / Cu; K2CO3 / decane / 24 h / 173 °C View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 20 p. 2548 - 2552