栎精-3,7,3’,4’-四甲醚合成路线 （共 31 条）
反应条件
potassium carbonate in acetone T=0°C; 3 h; Inert atmosphereReflux;
参考文献
EP2112145 A1, ;
Page/Page column 13 ;
反应条件
sodium carbonate in N,N-dimethyl-formamide T=20°C; 10 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 54, # 47 p. 6345 - 6348
反应条件
potassium carbonate in methanol; acetonitrile T=60°C; 10 h;
参考文献
Tetrahedron Letters, , vol. 43, # 26 p. 4617 - 4620
反应条件
silver(l) oxide in dichloromethane T=40°C; 4 h;
参考文献
Tetrahedron, , vol. 68, # 12 p. 2671 - 2678
反应条件
potassium carbonate in N,N-dimethyl-formamide T=25°C; 12 h; Inert atmosphere;
参考文献
European Journal of Medicinal Chemistry, , vol. 54, p. 210 - 222
反应条件
boron tribromide in dichloromethane T=0°C; 0.5 h;
参考文献
Tetrahedron, , vol. 60, # 11 p. 2647 - 2655
反应条件
aluminum tri-bromide in acetonitrile T=0°C; 1.5 h;
参考文献
Tetrahedron, , vol. 60, # 16 p. 3581 - 3592
反应条件
potassium hydroxide in water; acetone
参考文献
Magnetic Resonance in Chemistry, , vol. 47, # 12 p. 1043 - 1054
反应条件
1,4-dioxane; diethyl ether
参考文献
Journal of the American Chemical Society, , vol. 53, p. 4408
反应条件
1: 97 percent / K2CO3 / acetone / 2 h / Heating 2: 86 percent / dimethyl dioxirane / acetone; CH2Cl2 / 0.5 h / 0 - 20 °C 3: 96 percent / K2CO3 / acetone / 1 h / Heating 4: 99 percent / BBr3 / CH2Cl2 / 0.5 h / 0 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 11 p. 2647 - 2655
