(3S)-噁烷-3-甲醇合成路线 （共 52 条）
反应条件
water; copper on zirconia T=284 - 340°C; P=41372.9 Torr; 3 h; Product distribution / selectivity;
参考文献
EP1431296 A1, ;
Page 15-16 ;
反应条件
pyridine in dichloromethane T=20°C; 3.25 h;
参考文献
ABBOTT LABORATORIES
Patent: WO2009/67613 A1, 2009 ;
Location in patent: Page/Page column 103-104 ;
WO 2009/067613 A1
反应条件
triethylamine in tetrahydrofuran; hexane; acetone
参考文献
Mitsui Toatsu Chemicals, Inc.
Patent: US5614527 A1, 1997 ;
反应条件
1: pyridine / 0 - 20 °C 2: 7.18 g / dimethylformamide / 4 h / 80 °C View Scheme
参考文献
SUMITOMO CHEMICAL COMPANY, LIMITED; MIYAZAKI, Hiroyuki; MATSUO, Noritada; OHSHITA, Jun
Patent: WO2013/47904 A1, 2013 ;
反应条件
hydrogen; Catalyst C prepared in Example C (nickel on mixed silica-zirconia support Zr:Si:Ni 10:28:1) in water
T=280°C; P=10336 Torr; 1 h; Product distribution / selectivity;
参考文献
EASTMAN CHEMICAL COMPANY
Patent: EP1354881 A1, 2003 ;
Location in patent: Page/Page column 6-7 ;
反应条件
hydrogen; Criterion Catalyst 424 (C-424) comprising 3.0-4.5 weight percent nickel on alumina modified with phosphorus (6.0-9.0percent) and molybdenum (16.5-22.5percent) oxides in water
T=280 - 300°C; P=10336 - 41329.1 Torr; 1 h; Product distribution / selectivity;
参考文献
EASTMAN CHEMICAL COMPANY
Patent: EP1354881 A1, 2003 ;
Location in patent: Page/Page column 6-7 ;
反应条件
hydrogen; Catalyst G prepared in Example G (nickel on mixed silica-alumina Al:Si:Ni 1:1:1) in water
T=280°C; P=10336 Torr; 1 h; Product distribution / selectivity;
参考文献
EASTMAN CHEMICAL COMPANY
Patent: EP1354881 A1, 2003 ;
Location in patent: Page/Page column 6-7 ;
反应条件
water; copper on zirconia
T=250 - 370°C; P=40804.1 Torr; 3 h; Product distribution / selectivity;
参考文献
EASTMAN CHEMICAL COMPANY
Patent: EP1431296 A1, 2004 ;
Location in patent: Page 5-6 ;
反应条件
water; copper on zirconia
T=284 - 340°C; P=41372.9 Torr; 3 h; Product distribution / selectivity;
参考文献
EASTMAN CHEMICAL COMPANY
Patent: EP1431296 A1, 2004 ;
Location in patent: Page 15-16 ;
反应条件
1: With 4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=0 - 20°C;
2: With sodium hydrogencarbonate in dichloromethane; water
0.25 h;
参考文献
RECORDATI S.A.
Patent: WO2004/7418 A1, 2004 ;
Location in patent: Page 9-14 ;
