(3S)-噁烷-3-甲醇合成路线 （共 52 条）
反应条件
sodium tetrahydroborate; air; bis(dimethylglyoximato)pyridinecobaltate(I) ion Yield given. Multistep reaction;
参考文献
Okabe, Masami; Tada, Masaru
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 5 p. 1498 - 1503
反应条件
sodium tetrahydroborate; air; bis(dimethylglyoximato)pyridinecobaltate(I) ion Yield given. Multistep reaction;
参考文献
Okabe, Masami; Tada, Masaru
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 5 p. 1498 - 1503
反应条件
1H-imidazole; iodine; triphenylphosphine in dichloromethane T=0 - 25°C; 3.5 h;
参考文献
Berthel, Steven Joseph; Kester, Robert Francis; Murphy, Douglas Eric; Prins, Thomas Jay; Ruebsam, Frank; Sarabu, Ramakanth; Tran, Chinh Viet; Vourloumis, Dionisios
Patent: US2008/21032 A1, 2008 ;
Location in patent: Page/Page column 79 ;
US 20080021032 A1
反应条件
triethylamine in dichloromethane T=0 - 20°C; 36 h;
参考文献
UNIVERSITY COLLEGE CARDIFF CONSULTANTS LIMITED; REGA FOUNDATION
Patent: WO2004/96813 A1, 2004 ;
Location in patent: Page 37 ;
反应条件
triethylamine in dichloromethane 20 h;
参考文献
ELI LILLY AND COMPANY
Patent: WO2005/66126 A1, 2005 ;
Location in patent: Page/Page column 68 ;
WO 2005/066126 A1
反应条件
hydrogen; Catalyst C prepared in Example C (nickel on mixed silica-zirconia support Zr:Si:Ni 10:28:1) in water T=280°C; P=10336 Torr; 1 h; Product distribution / selectivity;
参考文献
EASTMAN CHEMICAL COMPANY
Patent: EP1354881 A1, 2003 ;
Location in patent: Page/Page column 6-7 ;
反应条件
hydrogen; Criterion Catalyst 424 (C-424) comprising 3.0-4.5 weight percent nickel on alumina modified with phosphorus (6.0-9.0percent) and molybdenum (16.5-22.5percent) oxides in water T=280 - 300°C; P=10336 - 41329.1 Torr; 1 h; Product distribution / selectivity;
参考文献
EASTMAN CHEMICAL COMPANY
Patent: EP1354881 A1, 2003 ;
Location in patent: Page/Page column 6-7 ;
反应条件
hydrogen; Catalyst G prepared in Example G (nickel on mixed silica-alumina Al:Si:Ni 1:1:1) in water T=280°C; P=10336 Torr; 1 h; Product distribution / selectivity;
参考文献
EASTMAN CHEMICAL COMPANY
Patent: EP1354881 A1, 2003 ;
Location in patent: Page/Page column 6-7 ;
反应条件
aluminium T=310 - 330°C; 0.5 h; Yield given. Yields of byproduct given;
参考文献
Infarnet, Yves; Accary, Armand; Huet, Jean
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 5-6 p. 261 - 266
反应条件
1.1: pyridine / 4 h / Inert atmosphere; Cooling with ice 2.1: potassium iodide / N,N-dimethyl-formamide / 3 h / 80 °C / Inert atmosphere 3.1: hydrazine hydrate / ethanol / 6 h / 70 °C / Inert atmosphere 3.2: Raney nickel / 4 h / 60 °C View Scheme
参考文献
SUMITOMO CHEMICAL COMPANY, LIMITED; MIYAZAKI, Hiroyuki; MATSUO, Noritada; OHSHITA, Jun
Patent: WO2013/47904 A1, 2013 ;
