暂无反应条件数据

1: toluenesulfonic acid / toluene / 1 h / Heating 2: 78 percent / S-Selectride / tetrahydrofuran / 23 h / Heating View Scheme

sodium hydrogencarbonate in chloroform; water

1: With hydrogen; palladium on activated carbon in water; isopropyl alcohol T=20°C; P=620.594 Torr; 24 h; 2: With sodium hydroxide in water; isopropyl alcohol T=0 - 5°C; pH=9 - 10; 1 h; Product distribution / selectivity;

sodium dithionite; ammonia; water T=70°C; pH=~ 6 - ~ 9; 17 h; Purification / work up;

1: With 1-chloroethyl chlorocarbonate; sodium carbonate in DCM 24 h; Heating / reflux; 2: With water in tetrahydrofuran; DCM T=20°C;