1: dimethyl lt;1-(methoxycarbonyl)ethylgt;phosphonate With sodium hydride in tetrahydrofuran; mineral oil
T=0 - 40°C; Horner-Wadsworth-Emmons olefination;
2: pelargonaldehyde in tetrahydrofuran; mineral oil
Horner-Wadsworth-Emmons olefination; 24 h; Reflux;
3: With platinum(IV) oxide; hydrogen in methanol
参考文献
Nawrath, Thorben; Gerth, Klaus; Mueller, Rolf; Schulz, Stefan
Chemistry and Biodiversity, 2010 , vol. 7, # 9 p. 2228 - 2253
Mastagli
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1937 , vol. 204, p. 1656
Annales de Chimie (Cachan, France), 1938 , vol. <11> 10, p. 281,369