反应条件
I2 in tetrachloromethane
under N2, dropwise addn. of I2 in CCl4 to a soln. of the Sn compound inCCl4 at 60°C, disappearance of violet colour; concg. the soln. after complete addn., pptn. recrystn. (petroleum ether(40 - 60°));
参考文献
Srivastava, P. C.; Srivastava, S. K.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1984 , vol. 23, # 9 p. 776 - 777
