hydrogen; palladium on activated charcoal in ethyl acetate P=2585.7 Torr; 5 h; Ambient temperature;

1: 89 percent / ammonium acetate, acetic acid / toluene / Heating 2: ethanol; H2O / 5 h / Heating 3: acetic acid, hydrochloric acid, H2O / 84 h / Heating View Scheme

1: 89 percent / ammonium acetate, acetic acid / toluene / Heating 2: ethanol; H2O / 5 h / Heating 3: acetic acid, hydrochloric acid, H2O / 84 h / Heating 4: 89 percent / acetic anhydride / 4 h / Heating View Scheme

1: 89 percent / ammonium acetate, acetic acid / toluene / Heating 2: ethanol; H2O / 5 h / Heating 3: acetic acid, hydrochloric acid, H2O / 84 h / Heating 4: 89 percent / acetic anhydride / 4 h / Heating 5: Heating 6: LiAlH4 / diethyl ether / 3 h View Scheme

1: 89 percent / ammonium acetate, acetic acid / toluene / Heating 2: ethanol; H2O / 5 h / Heating 3: acetic acid, hydrochloric acid, H2O / 84 h / Heating 4: 89 percent / acetic anhydride / 4 h / Heating 5: Heating 6: LiAlH4 / diethyl ether / 3 h View Scheme

1: 89 percent / ammonium acetate, acetic acid / toluene / Heating 2: ethanol; H2O / 5 h / Heating 3: acetic acid, hydrochloric acid, H2O / 84 h / Heating 4: 89 percent / acetic anhydride / 4 h / Heating 5: 100 percent / Heating 6: 95 percent / LiAlH4 / diethyl ether / 3 h View Scheme

ammonium acetate; acetic acid in toluene Heating;

1: 89 percent / ammonium acetate, acetic acid / toluene / Heating 2: ethanol; H2O / 5 h / Heating 3: acetic acid, hydrochloric acid, H2O / 84 h / Heating 4: 89 percent / acetic anhydride / 4 h / Heating 5: Heating 6: LiAlH4 / diethyl ether / 3 h View Scheme