3,3’-二硫基二苯甲酸合成路线 （共 27 条）
反应条件
dihydrogen peroxide; iodine in ethyl acetate T=20°C; 0.5 h;
参考文献
Journal of the American Chemical Society, , vol. 132, # 12 p. 4466 - 4476
反应条件
1: 97 percent / DABCO / N,N-dimethyl-acetamide / 16 h / 20 °C 2: 97 percent / 1 h / 215 °C 3: 95 percent / KOH / ethanol; H2O / 3 h / Heating 4: aq. NaOH; spermine / 20 °C / pH 8.25 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 128, # 31 p. 10253 - 10257
反应条件
1: 97 percent / 1 h / 215 °C 2: 95 percent / KOH / ethanol; H2O / 3 h / Heating 3: aq. NaOH; spermine / 20 °C / pH 8.25 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 128, # 31 p. 10253 - 10257
反应条件
1: 95 percent / KOH / ethanol; H2O / 3 h / Heating 2: aq. NaOH; spermine / 20 °C / pH 8.25 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 128, # 31 p. 10253 - 10257
反应条件
sodium hydroxide; N,N'-bis(3-aminopropyl)-1,4-butanediamine T=20°C; pH=8.25;
参考文献
Journal of the American Chemical Society, , vol. 128, # 31 p. 10253 - 10257
反应条件
phosphorus; iodine; acetic acid
参考文献
Yakugaku Zasshi, , vol. 77, p. 963
Chem.Abstr., , p. 2792
反应条件
hydrogenchloride; zinc in acetic acid T=100°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 117, # 1 p. 107 - 126
反应条件
in water; acetonitrile pH=4.5; 96 h; ammonium acetate buffer;
参考文献
Chemical Communications, , # 42 p. 5301 - 5303
反应条件
hydrogenchloride; zinc
参考文献
Acta Pharmacologica et Toxicologica, , vol. 4, p. 199,201
反应条件
hydrogenchloride; zinc
参考文献
Chemische Berichte, , vol. 32, p. 1156
