1,3-二(2-甲氧基苯基)脲合成路线 （共 27 条）
反应条件
1: 1.1.2.2-tetrachloro-ethane; bromine 2: aqueous ammonia / 150 °C View Scheme
参考文献
Gen.Aniline Works
Patent: US1792156 , 1929 ;
Full Text Show Details
I.G.Farbenind.
Patent: DE523437 , 1928 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 460
反应条件
acetic anhydride; acetic acid T=90°C;
参考文献
Ingle; Gaidhane; Dutta; Naha; Sengupta
Journal of Carbohydrate Chemistry, 2006 , vol. 25, # 8-9 p. 661 - 671
反应条件
1: nitrobenzene; chlorine 2: aqueous NaOH-solution / 175 °C View Scheme
参考文献
I.G.Farbenind.
Patent: DE511468 , 1928 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 459
Full Text Show Details
Gen.Aniline Works
Patent: US1792156 , 1929 ;
反应条件
1: HNO3 2: aqueous NH3 View Scheme
参考文献
Kupetow; Wukolowa
Zhurnal Obshchei Khimii, 1954 , vol. 24, p. 698,701;engl.Ausg.S.707,709
反应条件
pyridine; 1,2-dichloro-ethane
参考文献
Imp.Chem.Ind.
Patent: US2093265 , 1932 ;
反应条件
caesium carbonate; (9,9-dimethyl-9H-xanthene-4,5-diyl)bis(bis(3,5-bis(trifluoromethyl)phenyl)phosphine); tris(dibenzylideneacetone)dipalladium(0) chloroform complex in 1,4-dioxane
T=100°C; 4 h;
参考文献
Sergeev; Artamkina; Beletskaya
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 12 p. 1741 - 1752
反应条件
sodium acetate; selenium in water; N,N-dimethyl-formamide
T=95°C; 10 h; atmospheric pressure;
参考文献
Wang, Xiaofang; Lu, Shiwei; Yu, Zhengkun
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 8 p. 929 - 932
反应条件
copper diacetate; palladium diacetate in 1,4-dioxane
P=760.051 Torr; Reflux;
参考文献
Guan, Zheng-Hui; Lei, Hao; Chen, Ming; Ren, Zhi-Hui; Bai, Yinjuan; Wang, Yao-Yu
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 489 - 496
反应条件
PEG-400; cerium(III) chloride; potassium iodide in water
0.2 h; microwave irradiation;
参考文献
Li, Zheng
Synthetic Communications, 2005 , vol. 35, # 17 p. 2325 - 2331
反应条件
0.266667 h; microwave irradiation;
参考文献
Sarveswari; Raja
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 2 p. 546 - 547
