4,4′-二甲氧基苯偶酰合成路线 （共 154 条）
反应条件
1: KOH / ethanol / 2 h / Heating 2: AcOH View Scheme
参考文献
Kanyonyo, Martial; Govaerts, Sophie J.; Hermans, Emmanuel; Poupaert, Jacques H.; Lambert, Didier M.
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 15 p. 2233 - 2236
反应条件
hydroxymethanesulfinic acid sodium salt in water; N,N-dimethyl-formamide T=100°C; 1.5 h;
参考文献
Harris, Alan R.; Mason, Timothy J.
Synthetic Communications, 1989 , vol. 19, # 3and4 p. 529 - 536
参考文献
van Alphen
Recueil des Travaux Chimiques des Pays-Bas, 1929 , vol. 48, p. 1116
反应条件
1: diethyl ether / Kochen des nach der Hydrolyse erhaltenen Reaktionsprodukts mit konz. wss. HCl, Toluol und amalgamiertem Zink 2: AlI3 / 120 °C View Scheme
参考文献
Sah
Journal of the Chinese Chemical Society (Peking), 1946 , vol. 13, p. 111,117
反应条件
benzene Behandeln des Reaktionsgemisches mit wss. Ammoniumsulfat-Loesung;
参考文献
Kegelman; Brown
Journal of the American Chemical Society, 1954 , vol. 76, p. 2711
反应条件
2: acetyl chloride View Scheme
参考文献
Tiffeneau; Orechow
Bulletin de la Societe Chimique de France, 1925 , vol. <4>37, p. 437
反应条件
pyridine hydrochloride T=220°C; 1.5 h;
参考文献
Secondo, Patrick; Fages, Frederic
Organic Letters, 2006 , vol. 8, # 7 p. 1311 - 1314
反应条件
hydrogen bromide in water; acetic acid 17 h; Reflux;
参考文献
Bui, Thanh-Tuan; Garreau-De Bonneval, Benedicte; Moineau-Chane Ching, Kathleen I.
New Journal of Chemistry, 2010 , vol. 34, # 2 p. 337 - 347
反应条件
ammonium chloride; zinc in tetrahydrofuran T=20°C; 1 h;
参考文献
Hekmatshoar, Rahim; Heravi, Majid M.; Beheshtiha, Yahya S.; Faridbod, Farnoosh
Monatshefte fur Chemie, 2002 , vol. 133, # 2 p. 195 - 197
反应条件
formic acid; triethylamine; RuCl[(1S,2S)-TsDPEN](η6-p-cymene) in N,N-dimethyl-formamide T=35°C; 48 h;
参考文献
Murata, Kunihiko; Okano, Kazuya; Miyagi, Miwa; Iwane, Hiroshi; Noyori, Ryoji; Ikariya, Takao
Organic Letters, 1999 , vol. 1, # 7 p. 1119 - 1121
